Autosorb iQ - Outgassing (monitor) - Status: Available
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Fully automated high-resolution gas sorption analyzer possessing three sample ports (analysis station) and four sample preparation ports (outgassing station). Includes a turbo-molecular drag pump and low-pressure transducers (10 and 1 Torr) for measurement of adsorption behavior at pressures required for low surface area measurements (requires krypton) and to observe the filling of micropores. One port is available as a chemisorption station, complete with a high-temperature (1100⁰C) furnace coupled with fan-assisted cooling, and a digital temperature controller for precise chemisorption measurements. Includes automated gas switching, in-situ and/or separated sample preparation. A vapor dosing option is available for both physi - and chemi- sorption analysis and features a 50°C thermostatted manifold chamber. Typical vapors include water, alcohols, and aromatics which can impact material characteristics, shelf life, performance, and stability. Also, our Autosorb iQ is integrated with a thermal conductivity detector (TCD) & cold trap option and includes electronic loop injection. TCD enables to perform temperature programmed methods TPR (temperature-programed reaction)/ TPD (temperature-programed desorption)/ TPO (temperature-programed oxidation) and pulse chemisorption analyses for use with a wide-range of gases. The included, automatic loop injector allows for easy pulse titration analyses as well as peak calibration activities. Users can view the current tool screen (available on campus or via VPN only): http://sf01.nrf.aux.eng.ufl.edu/0.mp4 |
Use Prerequisites
| Prerequisite | Description | Status |
|---|---|---|
| Computer Access | Requires computer access be setup | Check Your Status |
| Funding Source | Requires permission to an active funding source | Check Your Status |
| Work Plan | Requires a work plan be approved by PI and staff | Check Your Status |
| Agreement Form | Requires completed agreement form for equipment usage | Check Your Status |
| NRF Safety Training | Requires completion of safety training | Check Your Status |
| NRF Building Access | Requires issue of an id badge and entry badge and/or access level to be set. | Check Your Status |
| Equipment Training | Requires completion of equipment training | Check Your Status |
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